The syntheses of 1-N-((S)-4-amino-2-hydroxybutyryl)gentamicin C1 and 1-N-((S)-3-amino-2- hydroxypropionyl)gentamicin C1.

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The syntheses and biological properties of 1-N-(S-4-amino-2-hydroxybutyryl)-gentamicin B and 1-N-(S-3-amino-2-hydroxypropionyl)-gentamicin B.

The syntheses of 1-N-(S-4-amino-2-hydroxybutyryl)-gentamicin B and 1-N-(S-3-amino-2-hydroxypropionyl)-gentamicin B, designated sch 20287 and Sch 21420, respectively, by procedures similar to those developed by KAWAGUCHI and co-workers for the transformation of kanamycin A to amikacin are described. The in vitro microbiological properties of Sch 20287 and Sch 21420 are compared with amikacin, ge...

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{2-[(S)-({2-[(S)-1-Benzyl­pyrrolidine-2-carboxamido]phen­yl}(phen­yl)methyl­ene)amino]-4-hydroxy­butanoato-κ4 N,N′,N′′,O}nickel(II)

The central Ni atom of the title compound, [Ni(C(29)H(29)N(3)O(4))], is coordinated by three N atoms [Ni-N = 1.955 (2), 1.844 (2) and 1.872 (2) Å] and by one O atom [Ni-O = 1.862 (2) Å] in a pseudo-square-planar geometry. The conformation of the hydroxy-butanoate side chain is controlled by a strong intra-molecular hydrogen bond (H⋯O = 1.84 Å).

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Synthesis of N, N΄3, 4-Dialkylamino-1, 2, 5-Oxadiazoles

N, N΄-3, 4-di(methylamino)-1, 2, 5-oxadiazole (1f) was prepared by dehydration of N, N΄-3, 4-di(methylamino)glyoxime (2f) in aqueous potassium hydroxid at 170-180 ˚C. Under similar conditions N, N΄-3, 4-di(benzylamino)-1, 2, 5-oxadiazole (1c) and N, N΄-3, 4-di(isopropylamino)...

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S-2-(Adamant-1-yl)-4-methyl­phenyl N,N-dimethyl­thio­carbamate

The title compound, C(20)H(27)NOS, was obtained from the corresponding O-thio-carbamate. The structure features a C=O bond distance of 1.209 (2) Å and an sp(3)-hybridized S atom [C-S-C = 101.66 (1)°]. The steric bulk of the 1-adamantyl substituent on the 2-position of the aromatic ring is reflected in the S-C-C-C torsion angle [-7.5 (3)°].

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ژورنال

عنوان ژورنال: The Journal of Antibiotics

سال: 1974

ISSN: 0021-8820,1881-1469

DOI: 10.7164/antibiotics.27.889